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By FLOREY KLAUS

Profiles of Drug elements, Excipients and similar method vol 1. content material: entrance hide; Analytical Profiles of Drug elements, quantity 1; Copyright web page; Contents; AFFILIATIONS OF EDITORS, participants, AND REVIEWERS; FOREWORD; PREFACE; bankruptcy 1. Acetohexamide; bankruptcy 2. Chlordiazepoxide; bankruptcy three. Chlordiazepoxide Hydrochloride; bankruptcy four. Cycloserine; bankruptcy five. Cyclothiazide; bankruptcy 6. Diazepam; bankruptcy 7. Erythromycin Estolate; bankruptcy eight. Halothane; bankruptcy nine. Levarterenol Bitartrate; bankruptcy 10. Meperidine Hydrochloride; bankruptcy eleven. Meprobamate; bankruptcy 12. Nortriptyline Hydrochloride; bankruptcy thirteen. Potassium Phenoxymethyl Penicillin. bankruptcy 14. Propoxyphene HydrochlorideChapter 15. Sodium Cephalothin; bankruptcy sixteen. Sodium Secobarbital; bankruptcy 17. Triamcinolone; bankruptcy 18. Triamcinolone Acetonide; bankruptcy 19. Triamcinolone Diacetate; bankruptcy 20. Vinblastine Sulfate; bankruptcy 21. Vincristine Sulfate. summary: Profiles of Drug ingredients, Excipients and similar method vol 1

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United S t a t e s Phamnacopia XVIII, p . 113 (1970). 8. , Personal Communication. 9. , Personal Communication. 10. MacMullan, E . A . , Personal Communication. 51 G, 523 (1967). CYCLOSERINE J. Lamb 53 J. W. LAMB C OI; 1. 2. 3. 4. 5. 6. 7. 53 P h o t o m e t r i c S y s t e m References - 54 CYCLOSERINE 1. 1 Name, F o r z u l a , M o l e c u l a r W e i g h t Cycloserine is ~-4-amino-3isoxazolidone. ihite t o s l i g h t l y yellow, p r a c t i c a l l y o d o r l e s s c r y s t a l l i n e powder.

Minima were o b s e r v e d a t 218 and 295-6 nm5. The s p e c t r u m i s shown i n t h e p r o f i l e f o r c h l o r d i a z e p o x i d e 6 . 4 Mass Spectrum The mass spectrum of c h l o r d i a z e p o x i d e hydrochloride is i d e n t i c a l t o t h a t reported f o r chlordiazepoxide6. 5 activity . Optical Rotation C h l o r d i a z e p o x i d e h y d r o c h l o r i d e e x h i b i t s no o p t i c a l 43 L A. MacDONALD, A. F. MICHAELIS, AND B. 2. 6 M e l t i n g Range C h l o r d i a z e p o x i d e melts w i t h decomposition.

MacDONALD, A. F. MICHAELIS, A N D B. Z . 3 m i n u t e s , which i n d i c a t e s p o s s i b l e decomposition on t h e column. The s e n s i t i v i t y w a s r e p o r t e d t o b e 0 . 0 4 pg. 4 Direct S p e c t r o p h o t o m e t r i c A n a l y s i s Direct s p e c t r o p h o t o m e t r i c a n a l y s i s of c h l o r d i azepoxide h a s n o t been found t o be a p p l i c a b l e i f s i g n i f i c a n t q u a n t i t i e s of t h e known h y d r o l y t i c contaminants a r e p r e s e n t .

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